自動(dòng)微量?jī)A濁點(diǎn)測(cè)試儀

MPC-102

New Standard ASTM D6749

No Methanol

新標(biāo)準(zhǔn)ASTM D6749，無(wú)甲醛

MPC-102 series has been designed for automatic determination of Pour Point (PP) and Cloud Point (CP) with small specimen size and shorter test cycle time while securing better test precision than the conventional manual methods’. PP measurement is made utilizing a new ASTM test method, namely “Air Pressure Method”(*1), which yields eventually no bias against the conventional test method, repeatability/reproducibility of 1℃/2℃ and 2-3 times faster determinations. The epoc-making high accuracy justifies PP determination at 1℃ intervals, which can help increasing the yields in the process. The CP/PP mode executes a CP determination and then PP determination consecutively, which further improves the test throughput in the lab. In addition to liquid-cooled model MPC-102L, air-cooled model MPC-102A is available. Multiple-tests versions with 6 test heads and 3 test heads are also available for higher volume tests.

MPC-102系列自動(dòng)微量?jī)A濁點(diǎn)測(cè)試儀，采用微量法測(cè)試樣品的傾點(diǎn)，取樣量少，測(cè)定過(guò)程由計(jì)算機(jī)自動(dòng)完成，無(wú)需人工干預(yù)，測(cè)定速度快而結(jié)果準(zhǔn)確。測(cè)定樣品的同時(shí)可同時(shí)測(cè)定樣品的濁點(diǎn)。儀器進(jìn)行傾點(diǎn)測(cè)試時(shí)，沒(méi)有采用傳統(tǒng)的“傾斜法”，而采用了新的標(biāo)準(zhǔn)ASTM D6749 “空氣加壓法”。測(cè)試結(jié)果與ISO3016和ASTM D97是所描述的傾斜法完全一致。樣品的測(cè)試間隔為1℃/2℃，并同時(shí)連續(xù)測(cè)試2-3次，測(cè)試結(jié)果具有更好的重復(fù)性和再現(xiàn)性。

MPC系列有多種型號(hào)可選擇。MPC-102L是液冷型，MPC-102A是風(fēng)冷型。MPC-302適用于3樣品同時(shí)測(cè)試，MPC-602用于6樣品同時(shí)測(cè)試。

*1:ASTM D6749 on “Standard Test Method for Pour Point of Petroleum Products (Automatic Air Pressure Method)” ASTM D6749《石油產(chǎn)品傾點(diǎn)測(cè)定法(自動(dòng)空氣加壓法)》

HIGH PRECISION POUR POINT DETERMINATION: 高精度的傾點(diǎn)測(cè)定

The typical repeatability and reproducibility are 1℃ and 2℃ respectively, when PP is determined at 1℃ intervals.(*2) This high precision attributes to the patented Air Pressure method, in which the disturbance to the formation of wax crystal structure through the test process is kept at a minimal and consistent level. “氣壓法”可有效避免降溫過(guò)程中，樣品的蠟狀析出和冰晶體對(duì)結(jié)果的干擾，按1℃間隔測(cè)試樣品，精度更高。

*2:Precision information is for general samples such as diesel fuels, base oils and finished lube oils. 柴油，基礎(chǔ)油和調(diào)和潤(rùn)滑油。

POUR POINT AT 1℃ TESTING INTERVALS:

With this high precision, PP can be determined at 1℃ intervals for more precise process control, and therefore a considerable savings in the procss can be realized.儀器可按1℃間隔測(cè)試樣品，測(cè)試精度大于試驗(yàn)標(biāo)準(zhǔn)測(cè)試規(guī)定,可以保證試驗(yàn)結(jié)果的精度更高。（重復(fù)性：傾點(diǎn)±1℃ 或3℃（儀器可按傳統(tǒng)方式3℃間隔測(cè)試）；濁點(diǎn)：±1℃）

EASY AND QUICK PP/CP DETERMINATION:

Just set up a sample, select a test mode and then press the START key. The sample is cooled at the steepest possible rate without affecting the formation/growth of wax crystal, which has been known to be a critical factor for PP/CP determination. The test cycle time is typically 1/3 to 1/2 of that of the conventional tilting method’s.(*3) 選好樣品后，輸入測(cè)試參數(shù)，預(yù)期的傾/濁點(diǎn)數(shù)據(jù)，按下“開(kāi)始”鍵。儀器即可按標(biāo)準(zhǔn)自動(dòng)進(jìn)行測(cè)試，并輸出結(jié)果。

相較于傳統(tǒng)測(cè)試方式，“氣壓法”的效率更高，一般只要傳統(tǒng)方式的1/3 或 1/2的時(shí)間，就可以完成測(cè)試?？稍诙虝r(shí)間內(nèi)進(jìn)行多組測(cè)試。

*3:When a diesel fuel oil with PP of –32.5℃ is tested, the Air Pressure method took 45 minutes while the conventional tilting method took 140 minutes. Note that the Japan Industrial Standard defines PP in 2.5℃ increments 柴油的傾點(diǎn)一般在–32.5℃左右，按傳統(tǒng)方法測(cè)試，每隔2.5℃測(cè)試一次，一個(gè)測(cè)試過(guò)程需要140分鐘，而應(yīng)用“氣壓法”的測(cè)試過(guò)程只要45分鐘，效率更高。

EASY SAMPLE HANDLING: 采樣少，易操作

Since the required sample volume is a mere 4.5mL and the sample cup is a test-tube type removable jar, the sample handling is extremely easy.樣品僅需求4.5毫升，玻璃小型樣品杯是一個(gè)可取放的瓶狀試管，操作極其簡(jiǎn)單。

COMPACT DESIGN &ENERGY EFFICIENT:

Use of Peltier Cells for sample cooling/heating made this “mini” tester not only compact in design but energy efficient. Depending on the temperature range, either air, tap water or small chiller with anti-freeze suffices the cooling requirement. No methanol is required. 儀器整體為臺(tái)式結(jié)構(gòu)，體積小，占地少，儀器本體內(nèi)置半導(dǎo)體制冷源及加熱裝置。使用小型樣品杯，取樣量少，制冷迅速，效率很高。配合不同的冷浴介質(zhì)，用于不同的測(cè)量范圍。無(wú)需甲醛。

TANAKA Mini Pour/Cloud Point Tester, series MPC-102

SPECIFICATIONS:

TYPE:

Mini Pour Point(PP) and Cloud Point(CP) tester with sequential CP and PP measuring capability.

應(yīng)用“氣壓法”測(cè)試樣品傾點(diǎn)(PP)，濁點(diǎn)(CP)，或樣品的濁點(diǎn)(CP)+傾點(diǎn)(PP)的連續(xù)測(cè)定

Sample cooling and pre-heating by TED. 特有的半導(dǎo)體制冷/加熱設(shè)計(jì)。

TEST STANDARDS:適用標(biāo)準(zhǔn)

ASTM D6749/D97, ISO 3016 (PP), （傾點(diǎn)）

ASTM D2500, ISO 3015 (CP) （濁點(diǎn)）

SPECIMEN VOLUME（樣品量）: 4.5ml

MEASURING RANGE: (typical*) 測(cè)試范圍

1.MPC-102L(Liquid cooled model):（液冷型）

 +51℃ to - 40℃ with tap water of 20℃ （直接外接循環(huán)水冷，水溫約在20℃）

 +51℃ to - 65℃ with cooling liquid of -35℃ （外接循環(huán)制冷源，介質(zhì)溫度約在零下35℃）

2.MPC-102A(Air cooled model): （風(fēng)冷型）

 +51℃ to -30℃ (in 25℃ ambient) （環(huán)境溫度在25℃左右）

*:Sample viscosity, etc. affects on lowest temperature of the measuring range.

樣品本身的低溫運(yùn)動(dòng)粘度的性質(zhì)，限制了試驗(yàn)所需要zui低的測(cè)試溫度。

MEASUREMENT MODES: 測(cè)試模式

Selectable from various modes.可選擇多種測(cè)試模式

1.CP mode (0.1  or 1.0 ℃, selectable) 濁點(diǎn)測(cè)試模式（每隔0.1 或 1.0℃測(cè)試）

2.PP modes: Programmed by the user. Programmable傾點(diǎn)測(cè)試模式，按用戶要求組合

parameters are: 需要先選擇油品種類，再選擇測(cè)試溫度。

*Amount of applied air pressure for PP detection, to accommodate different sample types: L(low) for diesel fuels, H(high) for lube oils, VH(very high) and UH (ultra high) for residual fuels and similar samples. 按油品種類（L-柴油；H-潤(rùn)滑油；VH或 UH-重油/渣油）

*Testing intervals: 1.0℃, 2.5℃, or 3.0℃ 按溫度每隔1.0℃, 2.5℃, 或 3.0℃測(cè)試

(In total, 4x3=12 modes for PP.) 以上總計(jì)12種組合傾點(diǎn)測(cè)試模式

3.CP/PP modes: 濁點(diǎn)+傾點(diǎn)連續(xù)測(cè)試 （重復(fù)測(cè)試）

CP is determined and then PP. PP detection is programmable by the user with the same parameters as PP modes’. (12 modes in total.) 到檢測(cè)出傾點(diǎn)后，樣品被自動(dòng)加熱至與室溫一致，再次連續(xù)測(cè)試樣品，或再次按不同的模式測(cè)試樣品，尤其適用于科研場(chǎng)合。

SAMPLE AUTOMATIC PRE-HEATING:樣品自動(dòng)加熱

Automatic preheating at either +45℃ or EPP+10℃. (EPP=Expected Pour Point)

按試驗(yàn)方法對(duì)樣品預(yù)熱步驟的要求，儀器也包括了樣品預(yù)熱的功能。每次測(cè)試時(shí)，樣品會(huì)按要求被預(yù)熱到（45℃）或（預(yù)期傾點(diǎn)+10℃）

DISPLAY: （顯示）

Test parameters, EPP, bath temperature, sample temperature, PP, and CP displayed on VFD. Temperatures displayed in 0.1℃ increments.

VFD熒光屏，清晰顯示試驗(yàn)參數(shù)，冷浴溫度，樣品溫度，傾點(diǎn)，濁點(diǎn)，預(yù)期傾點(diǎn)等內(nèi)容。

溫度顯示精度0.1℃。

EPP SETTING: 預(yù)期傾點(diǎn)設(shè)定

EPP(Expected Pour Point) needs to be set prior to test Starts. 測(cè)試開(kāi)始時(shí)需要輸入預(yù)期傾點(diǎn)

SPECIMEN CUP: （樣品杯）

Cylindrical glass test jar with 4.5ml sample volume.

石英玻璃的小型樣品杯，每次試驗(yàn)只需要4.5ml的樣品

SENSORS: 傳感器

Compound type sensor assembly for PP and CP. 同一儀器既可以檢測(cè)傾點(diǎn)，也可以檢測(cè)濁點(diǎn)

PP detected by air pressure method(patented). （的）氣壓傳感器變化檢測(cè)傾點(diǎn)

CP detected photo-electrically.光電傳感器檢測(cè)濁點(diǎn)

PT100 temp. sensors. PT-100鉑電阻檢測(cè)溫度

SAMPLE COOLING RATE: 降溫速率

As standard, 4℃/min. till EPP+40℃, and 1℃/min. thereafter. Cooling profile is programmable.

按標(biāo)準(zhǔn)規(guī)定：在預(yù)期傾點(diǎn)+40℃以前，降溫速率4℃/min；在此以后，降溫速率1℃/min。

用戶也可以自行設(shè)定特殊的降溫曲線，便于科研應(yīng)用。

SAFETY SHUTDOWN: 安全保護(hù)

As hot side of TED reaches 60℃ while preheating, warning buzzer beeps and heating stops.

半導(dǎo)體熱面溫度達(dá)到（60℃），超過(guò)限定時(shí) ，儀器報(bào)警提示，并且自動(dòng)停機(jī)

DATA OUTPUT: 數(shù)據(jù)輸出

RS-232C 1 channel (for PC or Optional Printer)

標(biāo)準(zhǔn)RS-232C接口，1（可用于計(jì)算機(jī)聯(lián)機(jī)控制或外接打印機(jī)輸出）

DATA STRAGE 記錄保存

Last 50 test data are stored in RAM 記錄后50次試驗(yàn)結(jié)果，即使掉電，數(shù)據(jù)也不會(huì)丟失。

POWER REQUIREMENTS: （電源需求）

100, 120, 220,  or 240VAC 0.5kW

DIMENSIONS AND WEIGHT: （體積和重量）

230mmWx480mmDx385mmH, 20kg

ORDERING INFORMATION:

STANDARD ACCESSORIES: （標(biāo)準(zhǔn)附件）

1.Specimen Cup with Reflex Seal 樣品杯（帶反光貼片）	5 pcs
2.Spare Pressure Conducting Tube 導(dǎo)壓軟管	2 pcs
3. AC Power Cord, 3.0m (電源線	1 pc
4.Connecting Cables(set of 2) 連接線	1 set
5.Hose and clamps(MPC-102L) 軟管和夾具(液冷型)	1 set
6.Dripping Plate(MPC-102L)防滴盤(pán)(液冷型)	1 pc
7.Instruction manual使用說(shuō)明書(shū)	1 copy

OPTIONAL ACCESSORIES:       （選購(gòu)件1）

·Water Regulator with Pressure Gauge (MPC-102L, for Connecting Tap Water)   

循環(huán)泵組件 (MPC-102L,直接外接水冷專用)

·Chillers for -60℃ of Measurement: TANAKA TCU-40B (MPC-102L): or Neslab RTE-740(*1) or Julabo FP40-MC(*2)   *1:Made in USA. *2:Made in Germany

試驗(yàn)溫度要求-60℃（零下60℃）需要外接循環(huán)制冷源，推薦以下型號(hào)：

TANAKA TCU-40B（日本田中制）或RTE-740（美國(guó)制）或Julabo FP40-MC（德國(guó)制）

·Chiller for -45℃ of Measurement: Neslab RTE-7(*1)

試驗(yàn)溫度要求-45℃（零下45℃）需要外接循環(huán)制冷源，推薦以下型號(hào)：Neslab RTE-7（美國(guó)制）

·Printer, BS2-80TS (w/ AC Adapter and Connecting Cable) 打印機(jī)（帶電源和連接線）

·Built-in Clock Board （內(nèi)置時(shí)鐘板）

SUGGESTED SPARES FOR 2 YEARS: （選購(gòu)件2，2年維護(hù)）

1.Specimen Cup with Reflex Seal樣品杯（帶反光貼片）	20 pcs
2.Reflex Seal（反光貼片）	30 pcs
3.Pressure Conducting Tube導(dǎo)壓軟管	5 pcs
4.O-Ring set (G-35 and P-8) O型圈（G-35 +P-8）	2 sets